Membrane organic vapor separation technology is a low-energy separation technology that can meet the development requirements of high efficiency and pollution-free separation technology in the modern industry, especially in the petrochemical industry. In the 1990s, Dalian Institute of Chemicals undertook the “8th Five-Year Plan†major research project of the Chinese Academy of Sciences—separation technology of organic vapor membrane technology. It first developed organic vapor membranes and separators in China, and carried out industrialization in Ethylene Branch of Jilin Chemical Corporation. The experiment was successful and its technology reached the international advanced level. In 2002, the institute cooperated with Jilin Chemical Co., Ltd. to carry out the research on the separation and recovery process of methyl chloride membranes. The researchers solved a number of technical problems, such as process calculations and process design, and developed a number of technical problems on the basis of a large amount of data. A set of chlorine-methane membrane recovery equipment for organic silicon production has achieved good social and economic benefits.